Systematic Study of the Effect of Incorporation of Carbon Nanotubes into GexSe1-x Glass System

Grade Level at Time of Presentation

Senior

Major

Physics/ Applied Mathamatics

Minor

Astronomy

2nd Grade Level at Time of Presentation

Junior

2nd Student Major

Physics

2nd Student Minor

Data Science

Institution

Northern Kentucky University

KY House District #

69

KY Senate District #

23

Department

Dept. of Phy, Gly, and Engg, Technology

Abstract

We successfully synthesized GexSe1-x (x = 0.225) glass samples and doped the samples with commercially produced (Protein Mods) carbon nanotubes (CNTs). We investigated the glass transition temperature (Tg) using Modulated Differential Scanning Calorimetry (MDSC). The glass samples without the CNTs have a Tg of ~220°C and the Tg was found to be independent of starting materials from different suppliers as well as water-bath temperature. CNTs, being a very hygroscopic material as well as oxygen absorbing material, needed to be cleaned under vacuum with the hot water-bath. We found that the Tg decreases when 5% and 10 % CNTs by mass is added to the glass samples as compared to the base GexSe1-x glass. The decrease in Tg indicates the occurrence of an intermediate phase (reduced-stress glass phase) at lower temperature, which could be potentially useful in material science applications.

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Systematic Study of the Effect of Incorporation of Carbon Nanotubes into GexSe1-x Glass System

We successfully synthesized GexSe1-x (x = 0.225) glass samples and doped the samples with commercially produced (Protein Mods) carbon nanotubes (CNTs). We investigated the glass transition temperature (Tg) using Modulated Differential Scanning Calorimetry (MDSC). The glass samples without the CNTs have a Tg of ~220°C and the Tg was found to be independent of starting materials from different suppliers as well as water-bath temperature. CNTs, being a very hygroscopic material as well as oxygen absorbing material, needed to be cleaned under vacuum with the hot water-bath. We found that the Tg decreases when 5% and 10 % CNTs by mass is added to the glass samples as compared to the base GexSe1-x glass. The decrease in Tg indicates the occurrence of an intermediate phase (reduced-stress glass phase) at lower temperature, which could be potentially useful in material science applications.